i Gas-Phase Condensation of nanoparticles ~ nanoall - Nanotechnology Blog

2/16/09

Gas-Phase Condensation of nanoparticles

The process utilises a gas, which is typically inert, at pressures high enough to promote particle formation, but low enough to allow the production of spherical particles. Gas-phase condensation uses a vacuum chamber that consists of a heating element, the metal to be made into nano-powder, powder collection equipment and vacuum hardware. Metal is introduced onto a heated element and is rapidly melted. The metal is quickly taken to temperatures far above the melting point, but less than the boiling point, so that an adequate vapour pressure is achieved. Gas is continuously introduced into the chamber and removed by the pumps, so the gas flow moves the evaporated metal away from the hot element. As the gas cools the metal vapour, nanometer-sized particles form. These particles are liquid since they are still too hot to be solid. The liquid particles collide and coalesce in a controlled environment so that the particles grow to specification, remaining spherical and with smooth surfaces. As the liquid particles are further cooled under control, they become solid and grow no longer. At this point the nanoparticles are very reactive, so they are coated with a material that prevents further interaction with other particles (agglomeration) or with other materials.

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